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  1. Task 1
  2. 1. Prepare a sample of ethyl ethanoate and test its
  3. purity, demonstrating skilful application of the
  4. techniques you use
  5. (i.e. reflux and distillation using QuickfitTM apparatus,
  6. addition of chemicals to purify the ethyl ethanoate
  7. and testing its purity by measuring its boiling point
  8. and infrared spectrum and comparing with
  9. reference information).
  10. 2. Write a report detailing your production and testing
  11. of ethyl ethanoate in the laboratory. The report must:
  12. 3. Explain the scientific principles behind your practical
  13. work techniques
  14. 4. Give detailed conclusions from your practical work
  15.  
  16. 5. Identify factors that affect the yield and purity of
  17. ethyl ethanoate in your laboratory preparation and
  18. analyse how significant these factors are
  19. 6. Research and describe the industrial manufacture
  20. and testing of ethyl ethanoate, including raw
  21. materials, equipment and scale of production.
  22. 7. Compare the laboratory and industrial manufacture
  23. and testing of ethyl ethanoate, explaining principles,
  24. similarities and differences in the equipment and
  25. techniques used.
  26. 8. Analyse how relevant the factors you have identified
  27. as affecting yield and purity are in the industrial
  28. manufacture of ethyl ethanoate.
  29. 9. Analyse whether boiling point measurement and
  30. infrared spectroscopy are effective ways to assesS
  31. purity of a liquid, and draw a conclusion on whether
  32. other methods used industrially, such as
  33. chromatography, are more reliable.
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