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- Task 1
- 1. Prepare a sample of ethyl ethanoate and test its
- purity, demonstrating skilful application of the
- techniques you use
- (i.e. reflux and distillation using QuickfitTM apparatus,
- addition of chemicals to purify the ethyl ethanoate
- and testing its purity by measuring its boiling point
- and infrared spectrum and comparing with
- reference information).
- 2. Write a report detailing your production and testing
- of ethyl ethanoate in the laboratory. The report must:
- 3. Explain the scientific principles behind your practical
- work techniques
- 4. Give detailed conclusions from your practical work
- 5. Identify factors that affect the yield and purity of
- ethyl ethanoate in your laboratory preparation and
- analyse how significant these factors are
- 6. Research and describe the industrial manufacture
- and testing of ethyl ethanoate, including raw
- materials, equipment and scale of production.
- 7. Compare the laboratory and industrial manufacture
- and testing of ethyl ethanoate, explaining principles,
- similarities and differences in the equipment and
- techniques used.
- 8. Analyse how relevant the factors you have identified
- as affecting yield and purity are in the industrial
- manufacture of ethyl ethanoate.
- 9. Analyse whether boiling point measurement and
- infrared spectroscopy are effective ways to assesS
- purity of a liquid, and draw a conclusion on whether
- other methods used industrially, such as
- chromatography, are more reliable.
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